Murphy, J.R. orcid.org/0009-0004-3680-8842, Obeidi, M.A. orcid.org/0000-0003-4496-2167, Ahad, I.U. orcid.org/0000-0002-3802-6156 et al. (1 more author) (2025) Investigating the effect of wire drawing and heat treatment on the response of Ni50.9Ti49.1 R-phase actuators. Materials, 18 (21). 4931. ISSN: 1996-1944
Abstract
In this investigation, Ni50.9Ti49.1 wires cold rolled to 40% and straight annealed at 480 °C, 510 °C, and 550 °C, respectively, were heat treated to shape set these wires as helical springs and enhance their SME for use as electro-mechanical actuators. These spring actuators were heat treated at 350 °C, 400 °C, and 450 °C for 30, 60, and 90 min. The wires’ performance as actuators was assessed on a custom-built testing rig, which measured both the stroke and actuation time for each wire. Additionally, the wires were characterised experimentally by DSC, XRD, and nanoindentation. The final resulting properties of the R-phase transformation helical spring actuator are controlled by the competing mechanisms of dislocation annihilation, and precipitation of Ni4Ti3, as well as the prior thermomechanical treatment. The optimum conditions for actuator response in Ni50.9Ti49.1 40% cold-worked wires were a straight annealing temperature of 480 °C and shape-setting aging conditions of 450 °C for 60 min. These parameters result in the optimum combination of defect annihilation and density of precipitates, resulting in a high-stroke (56 mm), low-hysteresis (2.68 °C) actuator with an actuation time of 6 s.
Metadata
| Item Type: | Article |
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| Authors/Creators: |
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| Copyright, Publisher and Additional Information: | © 2025 by the authors. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
| Keywords: | shape memory effect; heat treatment; nitinol; actuators; cold work; R-phase |
| Dates: |
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| Institution: | The University of Sheffield |
| Academic Units: | The University of Sheffield > Faculty of Engineering (Sheffield) > Department of Materials Science and Engineering (Sheffield) |
| Date Deposited: | 10 Nov 2025 14:58 |
| Last Modified: | 10 Nov 2025 14:58 |
| Status: | Published |
| Publisher: | MDPI AG |
| Refereed: | Yes |
| Identification Number: | 10.3390/ma18214931 |
| Open Archives Initiative ID (OAI ID): | oai:eprints.whiterose.ac.uk:234285 |
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