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Nicholls, TP, Bourne, RA orcid.org/0000-0001-7107-6297, Nguyen, BN orcid.org/0000-0002-0254-025X et al. (2 more authors) (2021) On-demand electrochemical synthesis of tetrakisacetonitrile copper(I) triflate and its application in the aerobic oxidation of alcohols. Inorganic Chemistry, 60 (10). pp. 6976-6980. ISSN 0020-1669
Abstract
An on-demand electrochemical synthesis of copper(I) triflate under both batch and continuous flow conditions has been developed. A major benefit of the electrochemical methodology is that the only byproduct of the reaction is hydrogen gas, which obviates the need for workup and purification, and water is not incorporated into the product. Upon completion of the electrochemical synthesis, solutions are directly transferred or dispensed into reaction mixtures for the catalytic oxidation of benzyl alcohol with no requirement for workup or purification.
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On-Demand Electrochemical Synthesis of copper(I) Triflate and Its Application in the Aerobic Oxidation of Alcohols. (deposited 23 Jul 2024 12:00)
- On-demand electrochemical synthesis of tetrakisacetonitrile copper(I) triflate and its application in the aerobic oxidation of alcohols. (deposited 23 Apr 2021 15:08) [Currently Displayed]