Shi, X, Beake, BD, Liskiewicz, TW orcid.org/0000-0002-0866-814X et al. (2 more authors) (2019) Failure mechanism and protective role of ultrathin ta-C films on Si (100) during cyclic nano-impact. Surface and Coatings Technology, 364. pp. 32-42. ISSN 0257-8972
Abstract
Complex mechanical behavior with phase transformation and high brittleness limits the reliability of silicon-based microelectromechanical systems. Although very hard ultra-thin films are being considered as protective overcoats to improve the service life of substrate materials, their resistance to fatigue can be at least as important as hardness when exposed to cyclic loading. In this study repetitive nano-impact tests with a spherical diamond probe have been used to investigate the fatigue behavior and protective role of 5 and 80 nm tetrahedral amorphous carbon (ta-C) films on silicon. At the lowest load there was delamination of the 80 nm film but not for the 5 nm film. At higher loads failure involved lateral cracking of the silicon substrate. Single impact tests showed that this was preceded by ring and radial cracking. Changing contact pressure during the test provided further support for the degradation mechanism and the influence of phase transformation in the Silicon substrate. Under repetitive contact the thin film systems showed lower impact depth and greater impact cycles before substrate fracture than the uncoated Silicon. This is related to their enhanced load support which affects phase transformation in the substrate, with potentially delamination providing an additional impact energy dissipation mechanism.
Metadata
Item Type: | Article |
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Authors/Creators: |
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Copyright, Publisher and Additional Information: | © 2019 Published by Elsevier B.V. This is an author produced version of a paper published in Surface and Coatings Technology. Uploaded in accordance with the publisher's self-archiving policy. |
Keywords: | Nano-impact; Tetrahedral amorphous carbon; Ultrathin films; Silicon; Failure mechanism |
Dates: |
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Institution: | The University of Leeds |
Academic Units: | The University of Leeds > Faculty of Engineering & Physical Sciences (Leeds) > School of Mechanical Engineering (Leeds) > Institute of Functional Surfaces (Leeds) |
Depositing User: | Symplectic Publications |
Date Deposited: | 26 Apr 2019 10:59 |
Last Modified: | 26 Feb 2020 01:38 |
Status: | Published |
Publisher: | Elsevier |
Identification Number: | 10.1016/j.surfcoat.2019.02.082 |
Related URLs: | |
Open Archives Initiative ID (OAI ID): | oai:eprints.whiterose.ac.uk:145356 |