Gou, Q, Xu, S, Hao, F et al. (9 more authors) (2019) Full-scale pores and micro-fractures characterization using FE-SEM, gas adsorption, nano-CT and micro-CT: A case study of the Silurian Longmaxi Formation shale in the Fuling area, Sichuan Basin, China. Fuel, 253. pp. 167-179. ISSN 0016-2361
Abstract
Pore-fracture structure of shales is important to shale gas resource potential evaluation, exploration and development. However, investigations about the pore-fracture structure of shales were mainly focused on nano-submicron pores, while the contribution of micrometer-scaled pores and micro-fractures to pore system of shale reservoirs lack sufficient attention. Here, using a combination of field-emission scanning electronic microscopy (FE-SEM), gas adsorption (N2 and CO2) and CT scanning (Nano-CT and Micro-CT), the Longmaxi shale cored from JYA well, in the Fuling area, was selected to comprehensively evaluate the characteristics of the pore-fracture structure at different scales. The results show that there are diverse types of pores in the organic-rich shale, mainly consisted of organic pores, inorganic pores (interP pores and intraP pores) and micro-fractures. Many pores are ink bottle-shaped characterized by narrow necks and wide bodies, while some others are slit-shaped. Pore size range from 0.305 nm to 98.5 μm. Pores with diameter of 0.305–2 nm (micro-pores), 2–50 nm (meso-pores), 50 nm-2 μm (macro-pores) and 2–98.5 μm (micro-fractures) account for 33.59%, 36.28%, 14.04% and 16.09% of the total pore volume, respectively. Moreover, shale permeability and specific surface area were calculated to be 0.005 mD and 39.44 m2/g, respectively, based on the full-scaled pore splicing. About 92% of specific surface area is contributed by pores with diameter of 0.305–5 nm. Micro-fractures connect with each other and form net-shaped structure with great connectivity from observational results. The micro-fractures with size of 20–98.5 μm provide the main permeability (about 90%). Micro-pores and small meso-pores in shale reservoirs provide large adsorption space for adsorbed gas, while micro-fractures enhance the seepage capability of shale gas, which are favorable for shale gas accumulation.
Metadata
Item Type: | Article |
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Authors/Creators: |
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Keywords: | Shale, Full-scale pore structure, Nano-CT, Micro-CT, Sichuan Basin, |
Dates: |
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Institution: | The University of Leeds |
Academic Units: | The University of Leeds > Faculty of Environment (Leeds) > School of Earth and Environment (Leeds) |
Depositing User: | Symplectic Publications |
Date Deposited: | 24 Mar 2023 08:54 |
Last Modified: | 22 May 2023 13:24 |
Published Version: | http://dx.doi.org/10.1016/j.fuel.2019.04.116 |
Status: | Published |
Publisher: | Elsevier |
Identification Number: | 10.1016/j.fuel.2019.04.116 |
Open Archives Initiative ID (OAI ID): | oai:eprints.whiterose.ac.uk:194737 |