Austen, Lauren, Dugmore, Thomas Iain James, Matharu, Avtar Singh orcid.org/0000-0002-9488-565X et al. (1 more author) (2022) Byproduct Valorization:From Spent Coffee Grounds to Fatty Acid Ethyl Esters. JOURNAL OF CHEMICAL EDUCATION. ISSN 0021-9584
Abstract
A laboratory experiment was designed to provide students with an introduction to byproduct valorization by producing an analogue of biodiesel (fatty acid ethyl esters, FAEE) via lipid extraction and subsequent transesterification from spent coffee grounds (SCG). Valorization is the process of upgrading underutilized or discarded wastes or byproducts into chemicals, materials, and (bio)energy. Upon isolation of the intermediate and FAEE, students analyzed the respective spectroscopic characteristics using infrared and nuclear magnetic resonance spectroscopy as well as evaluated gas chromatography spectra that were provided. Associated green metrics for the reaction were determined to obtain a quantitative measure of the “greenness” of the experiment. In this laboratory experiment, students are introduced to key concepts such as whole systems thinking and the United Nations Sustainable Development Goals where they apply these frameworks to real-world problems such as consumption and waste disposal. In addition to providing a greener alternative to traditional methods for biodiesel analogue production from SCG by solvent alterations, this experiment demonstrates the value of waste that would otherwise be overlooked to generate products that can help reduce the continued use of finite fossil fuels.
Metadata
Item Type: | Article |
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Authors/Creators: |
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Copyright, Publisher and Additional Information: | © 2022 The Authors |
Dates: |
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Institution: | The University of York |
Academic Units: | The University of York > Faculty of Sciences (York) > Chemistry (York) |
Depositing User: | Pure (York) |
Date Deposited: | 09 Nov 2022 09:30 |
Last Modified: | 08 Jan 2025 00:12 |
Published Version: | https://doi.org/10.1021/acs.jchemed.2c00728 |
Status: | Published online |
Refereed: | Yes |
Identification Number: | 10.1021/acs.jchemed.2c00728 |
Open Archives Initiative ID (OAI ID): | oai:eprints.whiterose.ac.uk:193089 |