Seifert, D.U., Li, L. orcid.org/0000-0002-9565-9830, Lee, K.-Y. et al. (3 more authors) (2021) Processing and properties of translucent bismuth sodium titanate ceramics. Journal of the European Ceramic Society, 41 (2). pp. 1221-1229. ISSN 0955-2219
Abstract
Lead-free bismuth sodium titanate piezoceramics were processed by a solid-state route with a novel precursor approach. By carefully controlling the processing parameters and sintering atmospheres, translucent ceramics with pore-free, homogeneous microstructures with exceptionally low dielectric loss at elevated temperatures. The pore-free microstructure can influence the operating life of a dielectric device positively, since pores and other microstructural defects are usually responsible for material failures within devices. Synchrotron and surface X-ray diffraction experiments revealed a clear dependence of the crystal structure on sintering parameters and defect chemistry. Microstructural analysis showed a dependency of a secondary phase on the sintering atmosphere. The grain size could be adjusted using a shortened grinding process instead of using the common methods like increasing calcining or sintering temperature.
Metadata
Item Type: | Article |
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Authors/Creators: |
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Copyright, Publisher and Additional Information: | © 2020 Elsevier. This is an author produced version of a paper subsequently published in Journal of the European Ceramic Society. Uploaded in accordance with the publisher's self-archiving policy. Article available under the terms of the CC-BY-NC-ND licence (https://creativecommons.org/licenses/by-nc-nd/4.0/). |
Keywords: | Bismuth sodium titanate; Electrical properties; Processing; Structural properties; Lead-free |
Dates: |
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Institution: | The University of Sheffield |
Academic Units: | The University of Sheffield > Faculty of Engineering (Sheffield) > Department of Materials Science and Engineering (Sheffield) |
Funding Information: | Funder Grant number Engineering and Physical Science Research Council EP/L027348/1 |
Depositing User: | Symplectic Sheffield |
Date Deposited: | 08 Dec 2020 08:46 |
Last Modified: | 02 Feb 2022 07:26 |
Status: | Published |
Publisher: | Elsevier |
Refereed: | Yes |
Identification Number: | 10.1016/j.jeurceramsoc.2020.10.009 |
Open Archives Initiative ID (OAI ID): | oai:eprints.whiterose.ac.uk:168807 |