Grogan, Gideon James orcid.org/0000-0003-1383-7056, Bonfield, Holly, Mercer, Kayleigh et al. (14 more authors) (2019) The Right Light – De Novo Design of a Robust Modular Photochemical Reactor for Optimum Batch and Flow Chemistry. Chemphotochem. ISSN 2367-0932
Abstract
Having identified inconsistencies when repeating literature examples of photochemical transformations and difficulties recreating experimental setups, we devised several criteria that an ideal labscale reactor should achieve. Herein, we introduce a versatile photoreactor for high throughput screening, preparative scale batch reactions and continuous processing, all with a single light source. The reactor utilizes interchangeable arrays of pseudo-monochromatic high-power LEDs in a range of synthetically useful wavelengths, combined with excellent temperature control. Moreover, light intensity can be modulated in an accurate and straightforward manner. This system has subsequently been tested on a range of literature methodologies.
Metadata
Item Type: | Article |
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Authors/Creators: |
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Copyright, Publisher and Additional Information: | This is an author-produced version of the published paper. Uploaded in accordance with the publisher’s self-archiving policy. Further copying may not be permitted; contact the publisher for details. |
Dates: |
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Institution: | The University of York |
Academic Units: | The University of York > Faculty of Sciences (York) > Chemistry (York) |
Depositing User: | Pure (York) |
Date Deposited: | 29 Aug 2019 08:40 |
Last Modified: | 08 Feb 2025 00:34 |
Published Version: | https://doi.org/10.1002/cptc.201900203 |
Status: | Published online |
Refereed: | Yes |
Identification Number: | 10.1002/cptc.201900203 |
Open Archives Initiative ID (OAI ID): | oai:eprints.whiterose.ac.uk:150174 |