Turner, TD orcid.org/0000-0003-3776-2044, Nguyen, TTH, Nicholson, P et al. (4 more authors) (2019) A temperature-controlled single-crystal growth cell for the in situ measurement and analysis of face-specific growth rates. Journal of Applied Crystallography, 52 (Part 2). pp. 463-467. ISSN 0021-8898
Abstract
The design and construction of a growth cell for the precision measurement of face-specific single-crystal growth rates are presented. Accurate mechanical drawings in SolidWorks of the cell and individual components are provided, together with relevant construction models. A general methodology for its use in the measurement of single-crystal growth rates and their underpinning growth mechanism is presented and illustrated with representative data provided for the crystal growth of the {011} and {001} faces of RS-ibuprofen single crystals grown in ethanolic solutions. Analysis of these data highlights the utility of the methodology in morphological model development and crystallization process design.
Metadata
Item Type: | Article |
---|---|
Authors/Creators: |
|
Copyright, Publisher and Additional Information: | (c) 2019 International Union of Crystallography, all rights reserved. Reproduced in accordance with the publisher's self-archiving policy. https://doi.org/10.1107/S1600576719002048. |
Keywords: | single-crystal growth measurement; crystal growth kinetics; single-crystal growth cell; crystal habit; habit modification. |
Dates: |
|
Institution: | The University of Leeds |
Academic Units: | The University of Leeds > Faculty of Engineering & Physical Sciences (Leeds) > School of Chemical & Process Engineering (Leeds) |
Funding Information: | Funder Grant number EPSRC EP/I014446/1 |
Depositing User: | Symplectic Publications |
Date Deposited: | 08 Apr 2019 12:36 |
Last Modified: | 08 Apr 2019 12:36 |
Status: | Published |
Publisher: | International Union of Crystallography |
Identification Number: | 10.1107/S1600576719002048 |
Open Archives Initiative ID (OAI ID): | oai:eprints.whiterose.ac.uk:144644 |