Turner, TD orcid.org/0000-0003-3776-2044, Nguyen, TTH, Nicholson, P et al. (4 more authors) (2019) A temperature-controlled single-crystal growth cell for the in situ measurement and analysis of face-specific growth rates. Journal of Applied Crystallography, 52 (Part 2). pp. 463-467. ISSN 0021-8898
Abstract
The design and construction of a growth cell for the precision measurement of face-specific single-crystal growth rates are presented. Accurate mechanical drawings in SolidWorks of the cell and individual components are provided, together with relevant construction models. A general methodology for its use in the measurement of single-crystal growth rates and their underpinning growth mechanism is presented and illustrated with representative data provided for the crystal growth of the {011} and {001} faces of RS-ibuprofen single crystals grown in ethanolic solutions. Analysis of these data highlights the utility of the methodology in morphological model development and crystallization process design.
Metadata
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Copyright, Publisher and Additional Information: | (c) 2019 International Union of Crystallography, all rights reserved. Reproduced in accordance with the publisher's self-archiving policy. https://doi.org/10.1107/S1600576719002048. | ||||
Keywords: | single-crystal growth measurement; crystal growth kinetics; single-crystal growth cell; crystal habit; habit modification. | ||||
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Institution: | The University of Leeds | ||||
Academic Units: | The University of Leeds > Faculty of Engineering & Physical Sciences (Leeds) > School of Chemical & Process Engineering (Leeds) | ||||
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Depositing User: | Symplectic Publications | ||||
Date Deposited: | 08 Apr 2019 12:36 | ||||
Last Modified: | 08 Apr 2019 12:36 | ||||
Status: | Published | ||||
Publisher: | International Union of Crystallography | ||||
Identification Number: | https://doi.org/10.1107/S1600576719002048 |