Development of an open-ended microstrip stub apparatus and technique for the dielectric characterization of powders

A new apparatus and method to characterize the complex dielectric permittivity of powders is described. The apparatus and technique are used to determine the dielectric properties of detergent powder agglomerates at different conditions. The technique is based on the measurement of Scattering-parameters of an open circuit microstrip stub partly loaded with the test powder material. The scattering parameters relate the voltage waves incident on the ports of a microwave network to those reflected from the ports and can easily be measured with a vector network analyzer. A 3D finite element electromagnetic field simulation tool HFSS (High frequency structural simulator) is used to replicate the measured S-parameters and then extract the complex permittivity data from it. The method has been verified by measuring the dielectric properties of disks of known dielectric materials – specifically Duriod 5880 and Teflon. Results are in good agreement with manufacturer data sheets. The complex permittivity of a range of detergent powder agglomerates with different moisture levels, at ambient and elevated temperatures, has been determined using this technique. Results are consistent with predictions of how the water interacts with the different components of the detergent particles at these different conditions.